
12. From the Maths dialog box choose Selected Trace and then the '=' (equals)
sign.
13. The results of this specular data equation will be displayed in a new graph.
Transmission measurements (%T)
Note
Parameters activated by a radio button that are not specifically mentioned in the
following procedure should be set to 'Off' (e.g., the Signal-to-noise mode radio
button). These parameters will not affect the procedure.
1. Place the accessory cap in the 'S' position, and place the protruding reference
plate in position over the reflectance port. Use the metal clamp to hold the
reference cap in position.
2. Set the following parameters:
Cary tab
X mode: Mode
anometers
X mode: Start 700
X mode: Stop 400
Y mode: Mode %T
Y mode: Y min -5.00
Y mode: Y max 110.00
Scan controls: Ave time (s) 0.100
Scan controls: Data interval (nm) 1.000
Scan controls: Scan rate (nm/min)600.00
Options tab
SBW/Energy: Fixed SBW ON
SBW/Energy: SBW (nm) 2.00 (See note below)
SBW/Energy: Beam mode Double
SBW/Energy: Slit height Reduced
Source: Lamps UV-Vis
Source: Source changeover (nm) 350.0
Baseline tab
Correction
one
Autostore tab
File Storage: Storage Storage on (prompt at start)
Note
If you are performing a transmission measurement using the small spot mount,
click here
, for the procedure for collecting a baseline.
Note
When operating in the visible range, the maximum SBW value you should use
for a standard 10 mm square cuvette is 1.5 nm.
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